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赵昱玮1,盛雪1,唐超1,刘健1,刘秀华1▲,曹扬1,高其品2.高效液相色谱法测定保健食品五味子猴菇口服液中葛根素的含量[J].中国医药科学,2020,(1):31-34        基金项目:吉林省中医药科技项目(2019155);吉林省科技发展计划项目(20180623037TC)
高效液相色谱法测定保健食品五味子猴菇口服液中葛根素的含量
Determination of puerarin in health food schisandrae hericium erinaceus oral liquid by high performance liquid chromatography
  
DOI:
中文关键词:  高效液相色谱法;五味子猴菇口服液;葛根素;含量测定
英文关键词:High performance liquid chromatography; Schisandrae hericium erinaceus oral liquid; Puerarin; Determination of contents
作者单位
赵昱玮1,盛雪1,唐超1,刘健1,刘秀华1▲,曹扬1,高其品2 1. 吉林省吉测检测技术有限公司,吉林长春 130117;2. 长春中医药大学,吉林长春 130117 
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中文摘要:
      [摘要] 目的 采用高效液相色谱法测定保健食品五味子猴菇口服液中葛根素的含量,为进一步提高其质量控制提供依据。方法 采用 Agilent ZORBAX Eclipse Plus C18(4.6mm×250mm,5μm)色谱柱,以乙腈 -0.05%磷酸溶液为流动相,检测波长为 250nm。结果 葛根素在 8.48106 ~ 42.4053μg/mL 范围内与峰面积呈良好线性关系(r > 0.9990); 平均加样回收率(n=6)分别为 101.47%。结论 建立了五味子猴菇口服液中葛根素的含量测定的方法,方法重复性良好,为该保健食品的产品质量控制提供依据。
英文摘要:
      [Abstract] Objective To determine the contents of puerarin in health food schisandrae hericium erinaceus oral liquid by high performance liquid chromatography to provide the reference for further improving the quality control. Methods An Agilent ZORBAX Eclipse Plus C18 (4.6mm × 250mm, 5μm) column was used with acetonitrile -0.05% phosphoric acid as the mobile phase. The detection wavelength was 250nm. Results Puerarin showed a good linear relationship with the peak area in the range of 8.48106-42.4053μg/mL (r > 0.9990). The average sample recovery rate (n=6) was 101.47%. Conclusion The method for determination of puerarin in schisandrae hericium erinaceus oral liquid is established. The method has good repeatability and provides the basis for the quality control of the health food.
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